China Professional Supplier Methyl Amine HCl / Methylamin Hydrochloride with Fast Delivery CAS 593-51-1, Find details about China 593-51-1, Methylamin Hydrochloride from China Professional Supplier Methyl Amine HCl / Methylamin Hydrochloride with Fast Delivery CAS 593-51-1
Methylamin hydrochloride Chemical Properties |
Melting point | 231-233 °C(lit.) |
Boiling point | 225-230 °C15 mm Hg(lit.) |
density | 0.8306 (rough estimate) |
refractive index | 1.5500 (estimate) |
Fp | 225-230°C/15mm |
storage temp. | Store below +30°C. |
solubility | soluble |
form | powder |
color | White crystalline |
Odor | Odorless |
PH | 5-7 (10g/l, H2O, 20ºC) |
PH Range | 5 - 7 at 10 g/l at 20 °C |
Water Solubility | soluble |
Sensitive | Hygroscopic |
Merck | 14,6014 |
BRN | 3588822 |
Stability: | Stable, but may be moisture sensitive. Incompatible with strong oxidizing agents. |
InChIKey | NQMRYBIKMRVZLB-UHFFFAOYSA-N |
CAS DataBase Reference | 593-51-1(CAS DataBase Reference) |
NIST Chemistry Reference | Methylammonium chloride(593-51-1) |
EPA Substance Registry System | Methylamin hydrochloride (593-51-1) |
Safety Information |
Hazard Codes | Xn |
Risk Statements | 22-36/37/38 |
Safety Statements | 26-37/39 |
WGK Germany | 1 |
RTECS | PA0603000 |
F | 10 |
TSCA | Yes |
HS Code | 29211190 |
Methylamin hydrochloride Usage And Synthesis |
Chemical Properties | white to light tan solid |
Definition | ChEBI: The hydrochloride formed from methylamin. |
Preparation | Methylamin hydrochloride is prepared by heating a mixture of aqueous formaldehyde and ammonium chloride; the residual water and the produced in the reaction are removed via vacuum distillation. This leaves behind solid methylamin hydrochloride. The solid is then purified by organic extractions and additional vacuum distillations. Methylamin gas for the reaction with P2P is generated in situ by heating the hydrochloride salt. Alternatively, methylamin can be liberated from the hydrochloride with base and collected in a cold finger or flask immersed in a dry ice bath. |
Purification Methods | Crystallise the salt from, absolute EtOH or MeOH/CHCl3. Wash it with CHCl3 to remove traces of hydrochloride. Dry it under vacuum first with H2SO4 then P2O5. It is deliquescent; store it in a desiccator over P2O5. [Beilstein 4 IV 122.] |
Methylamin hydrochloride Preparation Products And Raw materials |
Preparation Products | 4-N-Boc-4-N-Methyl-aminopiperidine-->1-METHYL-1H-IMIDAZOLE-5-CARBOXALDEHYDE-->1-Boc-4-Methylaminopiperidine-->N-Methyl-1,2-benzenediamine dihydrochloride-->1-Methyl-4-(methylamino)piperidine-->2-(2-METHYLAMINOETHYL)PYRIDINE-->1-(4-HYDROXY-3-METHOXYPHENYL)-2-NITROETHENE-->N-METHYL-2-NITROANILINE-->Deferiprone-->1-Methyl-1-nitrosourea-->N,alpha-dimethylcyclohexaneethylamine-->DL-Methamphetamine-->4-Bromo-2-fluoro-N-methylbenzamide-->Hydroxy-PEG1-methylamin-->METHYL-(2-PIPERIDIN-1-YL-ETHYL)-AMINE-->3-[(methylamino)methyl]phenol-->4-METHYL-3-METHYLAMINOPYRIDINE |