China X Ray Diffractometer for Elemental Analyze, Find details about China X Ray Diffractometer, Diffractometer from X Ray Diffractometer for Elemental Analyze
D-Series X-ray diffractometers are mainly used in the analysis of power, massive or film samples with their qualitative/quantitative attributes, crystal structure, material structure, crystal orientation, micro and macro stress, size of crystal and crystallinity. | |||
Name | Major Technical Parameters | Characters | |
X-ray Generator (Imported PLC Technology) | Voltage(Single-phase) | AC 220V±10% | As taking the imported PLC technology, so it has the characters of high automation, low faulty rate, high resistance to noisy factors, high stability and long life for the whole system. PLC working with PC controls the on/off of the shutter and the current and voltage and self-trains the X tube. |
Rated power | 5KW | ||
Tube voltage | 10~60kV1kV /Step | ||
Tube current | 2~80mA,1mA /Step | ||
Stability | ≤0.005% | ||
High-pressure cable | Dielectric voltage: 100V, length: 2m. | ||
Goniometer | Structure | JF-2500(Horizontal) JF-3000(Vertical) JF-3500(Keep sample still) | Vertical sample,θ-2θ Horizontal sample,θ-2θ Horizontal sample,θS-θd |
Scanning radius | 185mm | The system of angle measurement takes the imported high-accuracy bearing transmission, upgrading the accuracy of the measurement to samples and extending the life of the instrument. The instrument also takes two types of optical system: the focusing one and the parallel one, both with the function of dynamic adjustment. The instrument takes the θ/2θ driving or θ-2θ working together, with continuous or step-in scanning. | |
Range of scanning (2θ) | -35~170°, | ||
Speed of scanning | 0.006~120°/min | ||
Repeating accuracy (2θ) | ≤0.0005° | ||
Min step-in angle | 0.0001° | ||
Accuracy | ≤0.001° | ||
Filter | Ni(for Cu target) | ||
Turning speed | 1500°/min | ||
Slit system | Auto adjustable slit system | ||
Recording Control Unit | counter | PC/SC(proportional/ Scintillation) | Recording control system, based on the technology of Panalytical diffractometer from Netherlands, applies the human-computer interface with touch screen and the advanced PLC controlling technology. The circuit of the system using the concept of modeling design greatly improves system's resistance to noisy signals, so the system achieves better stability. |
Linear range of counter | ≥10,000,000cps | ||
Max background noisy | ≤1cps | ||
High-pressure of the counter | 0~2100V adjustable | ||
Way of counting | In differential way and in integral way | ||
Stability in high voltage of detector | Better than±0.005% | ||
Resolution of spectroscopy | sc:≤50% pc:≤20% | ||
Recycled Refrigeration System | structure | Split-type or all-in-one | The recycled refrigeration system automatically controls the water temperature and displays the temperature of the X tube, with dynamically choosing the variety of temperature. As the instrument has its own recycled refrigeration system and stainless steel pumps, so there is no need for external cooling system and it reduces the noise and avoids watermarks, which always block the X-ray tube. |
Operating temperature | 0-50°C | ||
Operating voltage | 220V | ||
Precaution | Detecting flow pressure Detecting refrigerant pressure Protection of over-high/under-low temperature | ||
PC | Host | Dual core CPU/RAM2G/HD500G | Brand PC |
Monitor | 21″LCD | ||
Printer | Laser | ||
Protections | Warning settings | Warnings for: over-high KV,mA, under-low KV,mA, run out of water, high-temperature of x tube, over current of whole equipment, power warning for x tube etc. | 5 scales of power protection: 0.8,1.2,1.8,2.2,2.7 |
Security settings | Double protected system/ shutter window and lead door working together/shutter window will be closed automatically while lead door opens | ||
Leakage of x-ray | Inspection based on <GBZ115-2002 Hygiene Protection Standards of x-ray Diffraction and Fluorescence Analyzer >. Radiation Safety Permit No.: 00150] Rays measurement outside the shield:≤0.1μSv/h | Applying the high-density and high-transparent lead glass for the protection. | |
Software | Controlling software | 1.Chinese interface on Windows platform with functions of controlling the voltage and current in x-ray generator and aging training of the shutter and x tube 2. Automatically controlling the diffractometer to scan the sample in steps way or in continuous way while sampling; automatically making the goniometer step forward/backward and adjusting the goniometer to 2θ | |
Application | 1. Smooth, fit/remove background, peel off Kα2 2. Searching peaks (marking peaks: value of D, 2θstrength, width of half-height, value of 2θand displaying all parameters ) 3. Change stepsize of sampling, removing noisy peaks; adjusting value of d and positions of peaks 4. Calculat integral area, integral width, width of half-height, comparison of patterns, integration of patterns. 5. Add text in patterns; two cursors: small cursor and big cursor. 6. Variety of zooming, variety of coordinates: linear, logarithm, square root 7. Put pictures in clipboard or paste into word/excel 8. Program for recognizing peaks, calculation of crystallinity, refining the parameters of crystal cell, standardization; quantitative analysis of clay | Details in : "Data Processing" in "JF Seriess of X-ray Diffractometer" | |
Curved Graphite Crystal Monochromator (optional) | Reflection | η>=30% | Applying this optional to the instrument will upgrade the comparison of different peaks and greatly recognize the weak peaks and reduce the diffraction angle of the diffractometer. |
Gradient of crystal surface | ±2 ° | ||
Mosaic degrees | <=0.55 | ||
Target material | Cu | ||
China-made X-ray Tube | Power | 2kW | |
Focus | 1×10mm | ||
Target | One Cu target |